Efficiency of Silver nanoparticles (AGNPS) synthesis based on sample preparation of mangrove baitworm (Annelida Eunicidae) Marphysa moribidii Idris hutchings and Arshad 2014


Citation

Izwandy Idris, . and Mohammad Asyraf Adhwa Masimen, . and Wan Iryani Wan Ismail, . and Umi Sharifah Nadhirah Ibrahim, . and Noor Aniza Harun, . Efficiency of Silver nanoparticles (AGNPS) synthesis based on sample preparation of mangrove baitworm (Annelida Eunicidae) Marphysa moribidii Idris hutchings and Arshad 2014. pp. 84-98. ISSN 2672-7226

Abstract

Green synthesis of silver nanoparticles (AgNPs) is gaining interest due to its environmentally friendly easy and biocompatible process. AgNPs synthesis using polychaete extract is relatively new but exhibits good potential. This study examines a local baitworm species Marphysa moribidii on its efficiency in synthesising AgNPs using two-sample preparations (fresh and frozen) with different weights. Samples were mixed with silver nitrate (AgNO3 ) before recording the colour changes. The ultraviolet-visible (UV-Vis) spectroscopy analysis scanning electron microscope (SEM) and transmission electron microscope (TEM) were undertaken to detect the quantity and quality of synthesised AgNPs. Successful synthesis of AgNPs was observed for both samples as the solution colour changed from pinkish red to brown and confirmed with surface plasmon resonance peaks. Fresh extract with 5 g 10 g and 15 g demonstrated higher reducing capability in AgNP synthesis than those frozen based on their peak uniformity in the UVVis spectrum. SEM and TEM images revealed spherical AgNP formation which is the preferred shape for antimicrobial studies. X-ray diffraction and Fourier transform infrared spectroscopy found no trace of Ag contaminants from the environment. Further analysis and optimisation are required to reveal the reducing mechanism especially using fresh samples as it has a higher capability in synthesising AgNPs.


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Abstract

Green synthesis of silver nanoparticles (AgNPs) is gaining interest due to its environmentally friendly easy and biocompatible process. AgNPs synthesis using polychaete extract is relatively new but exhibits good potential. This study examines a local baitworm species Marphysa moribidii on its efficiency in synthesising AgNPs using two-sample preparations (fresh and frozen) with different weights. Samples were mixed with silver nitrate (AgNO3 ) before recording the colour changes. The ultraviolet-visible (UV-Vis) spectroscopy analysis scanning electron microscope (SEM) and transmission electron microscope (TEM) were undertaken to detect the quantity and quality of synthesised AgNPs. Successful synthesis of AgNPs was observed for both samples as the solution colour changed from pinkish red to brown and confirmed with surface plasmon resonance peaks. Fresh extract with 5 g 10 g and 15 g demonstrated higher reducing capability in AgNP synthesis than those frozen based on their peak uniformity in the UVVis spectrum. SEM and TEM images revealed spherical AgNP formation which is the preferred shape for antimicrobial studies. X-ray diffraction and Fourier transform infrared spectroscopy found no trace of Ag contaminants from the environment. Further analysis and optimisation are required to reveal the reducing mechanism especially using fresh samples as it has a higher capability in synthesising AgNPs.

Additional Metadata

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Item Type: Article
AGROVOC Term: Biosynthesis
AGROVOC Term: Antimicrobials
AGROVOC Term: Annelida
AGROVOC Term: Spectroscopy
AGROVOC Term: Ultraviolet spectrophotometry
AGROVOC Term: Scanning microscopy
AGROVOC Term: Chemical composition
AGROVOC Term: Antimicrobial properties
AGROVOC Term: Growth inhibition
Depositing User: Mr. AFANDI ABDUL MALEK
Last Modified: 24 Apr 2025 00:55
URI: http://webagris.upm.edu.my/id/eprint/10737

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